HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-dimethyl-m-phenylenediamine → HCID 66670065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-dimethyl-m-phenylenediamine | HCID 76084 | — |
| Reactant | 6-chloro-N-methylpyrimidin-4-amine | HCID 309479 | — |
| Product | HCID 66670065 | HCID 66670065 | — |
Reaction Steps
The title compound is prepared analogously as described in Example 105A from (6-chloro-pyrimidin-4-yl)-methylamine and N,N-dimethyl-m-phenylenediamine. The crude product obtained after evaporation of the ethyl acetate layer is purified by flash chromatography (CH2Cl2/CH3OH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08552002B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-22968072f82548bab1670855f6e41894 |
| Source note | uspto-grants-2013_10 |