m-Toluidine → (3-Aminobenzyl)diethylamine

HRID 1038739Notes

Reaction equation

HRID 1038739 reaction equation
[CH2:1]([N:3]([CH2:14][CH3:15])[CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([N+:11]([O-])=O)[CH:6]=1)[CH3:2].CC1C=C(C=CC=1)N>>[CH2:1]([N:3]([CH2:4][C:5]1[CH:6]=[C:7]([NH2:11])[CH:8]=[CH:9][CH:10]=1)[CH2:14][CH3:15])[CH3:2]

Participants

3

Reactant 2

HCID 7934m-ToluidineHCID 5307027HCID 5307027, compound

Product 1

HCID 3359246(3-Aminobenzyl)diethylamine

Procedure

The title compound is prepared as described in Example 149B but using diethyl-(3-nitrobenzyl)-amine. The title compound contains 30% of 3-methyl-aniline and is used as a crude impure material.

Workup

  1. customThe title compound is prepared

Sources & evidence

ORD record
ord-63acc0155e514fec9900f7c0282d0074
Source dataset
uspto-grants-2013_10
Patent number
US08552002B2

Reaction notes

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