HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanoic acid → Butyl benzenepropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanoic acid | HCID 107 | — |
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | Butyl benzenepropanoate | HCID 568855 | — |
Reaction Steps
Under a nitrogen atmosphere, a mixture of 3-phenylpropionic acid (3.0 mmol), n-butanol (3.6 mmol), the zinc cluster obtained in the above-described Example 1 (0.0375 mmol), and diisopropyl ether (5.0 ml) was refluxed for 18 hours. As a result, butyl 3-phenylpropionate was obtained quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08552204B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-ed5621dc8bd24dc8a8320ecf745508b5 |
| Source note | uspto-grants-2013_10 |