HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1039990Generated: October 30, 2026
p-Toluenesulfonic acid → HCID 67256257, compound
https://huagongshe.com/reaction/1039990
Participants
| Role | Name | HCID | Charge |
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| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | 2-Chloro-4-(trifluoromethyl)pyrimidine | HCID 2773912 | — |
| Reactant | 3-Bromo-4-fluoroaniline | HCID 2779286 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67256257 | HCID 67256257 | 89.3% |
Reaction Steps
To 3-bromo-4-fluoroaniline (0.76 g, 4.0 mmol) and 2-chloro-4-(trifluoromethyl)pyrimidine (0.73 g, 4.0 mmol) was added dioxane (13.33 mL) and p-TSA (0.761 g, 4.0 mmol). The reaction was sealed and was heated at reflux overnight. The reaction was cooled to room temperature and was diluted with ethyl acetate, washed with saturated aqueous NaHCO3, and the organic was dried over sodium sulfate and filtered before concentration. The crude product was purified by flash chromatography (25:75 ethyl acetate:hexanes) to afford N-(3-bromo-4-fluorophenyl)-4-(trifluoromethyl)pyrimidin-2-amine (1.2 g, 3.57 mmol, 89%) as a pale yellowish solid. 1H NMR (500 MHz, CDCl3): δ 8.68 (d, J=4.9 Hz, 1H); 7.99-7.96 (m, 1H); 7.51 (d, J=8.4 Hz, 1H); 7.29 (s, 1H); 7.14 (t, J=8.5 Hz, 1H); 7.10 (d, J=4.9 Hz, 1H). rhSYK activity=+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08551984B2 |
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| Source dataset | uspto-grants-2013_10 |
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| ORD ID | ord-346682386d324493a54da1e8e54d8695 |
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| Source note | uspto-grants-2013_10 |
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