HCID 87169893, compound → HCID 66553530, compound

Participants

Reaction Steps

To a suspension of [1R,2R]toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-2-methyl-propyl)-phenyl ester oxalate salt (2 g) in dichloromethane (10 ml), 2N hydrochloric acid (2.7 ml) was added and stirred for 30 minutes. Layers were separated and organic layer was washed with water. Solvent was distilled off from the organic layer to give 1.29 g of the title compound having purity 98.2% by HPLC.

Provenance & Evidence