HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylphenyl boronic acid → HCID 66720830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylphenyl boronic acid | HCID 2733267 | — |
| Reactant | HCID 86637362 | HCID 86637362 | — |
| Product | HCID 66720830 | HCID 66720830 | 95% |
Reaction Steps
According to the method described in example 4.5, starting from 1.5 g (2.99 mmol) of methyl 5-[3-(benzyloxy)-4-chlorophenyl]-6-{[(trifluoromethyl)sulphonyl]oxy}nicotinate and of 508 mg (3.74 mmol) of 2-methylphenyl boronic acid, we obtain 1.26 g of methyl 5-[3-(benzyloxy)-4-chlorophenyl]-6-(2-methylphenyl)nicotinate in the form of oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08552201B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-995c5065d5394c0789f71e2e4bb16f5f |
| Source note | uspto-grants-2013_10 |