HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazinyl-4-iodopyridine → HCID 178453093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazinyl-4-iodopyridine | HCID 53402897 | — |
| Reactant | Tert-butyl (1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate | HCID 86654345 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178453093 | HCID 178453093 | — |
Reaction Steps
To tert-butyl (1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate (112 mg, 0.303 mmol) in DCM (20 mL) was added 1-(4-iodopyridin-2-yl)hydrazine (78.4 mg, 0.333 mmol). The reaction mixture was stirred for 1 hour and then taken on to directly to the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08557809B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-07166c0a1907496e8a191a1a6137e0bf |
| Source note | uspto-grants-2013_10 |