HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthalenesulfonic acid → HCID 44217414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthalenesulfonic acid | HCID 8420 | — |
| Reactant | 4SC-202 (free base) | HCID 15985904 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 44217414 | HCID 44217414 | 92.8% |
Reaction Steps
2.00 g (E)-N-(2-Amino-phenyl)-3-{1-[4-(1-methyl-1H-pyrazol-4-yl)-benzene sulfonyl]-1H-pyrrol-3-yl}-acrylamide was suspended in 40 mL isopropanol. 1.46 g naphthalene-2-sulfonic acid (70%) was added and the suspension was stirred for 24 h. The suspension was filtered, the filter cake was washed with 20 mL isopropanol and dried. An off-white solid (2.72 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08557858B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-600614db947a411d826bd597446c7a10 |
| Source note | uspto-grants-2013_10 |