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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1042366Generated: November 2, 2026

2-Naphthalenesulfonic acid → HCID 44217414, compound

https://huagongshe.com/reaction/1042366

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Naphthalenesulfonic acidHCID 8420—
Reactant4SC-202 (free base)HCID 15985904—
SolventIsopropanolHCID 3776—
ProductHCID 44217414HCID 4421741492.8%

Reaction Steps

2.00 g (E)-N-(2-Amino-phenyl)-3-{1-[4-(1-methyl-1H-pyrazol-4-yl)-benzene sulfonyl]-1H-pyrrol-3-yl}-acrylamide was suspended in 40 mL isopropanol. 1.46 g naphthalene-2-sulfonic acid (70%) was added and the suspension was stirred for 24 h. The suspension was filtered, the filter cake was washed with 20 mL isopropanol and dried. An off-white solid (2.72 g) was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08557858B2
Source datasetuspto-grants-2013_10
ORD IDord-600614db947a411d826bd597446c7a10
Source noteuspto-grants-2013_10