HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Diethyl-2-(3-methoxy-4-nitrophenoxy)ethylamine → HCID 59428024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Diethyl-2-(3-methoxy-4-nitrophenoxy)ethylamine | HCID 68463557 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59428024 | HCID 59428024 | — |
Reaction Steps
N,N-Diethyl-2-(3-methoxy-4-nitrophenoxy)ethylamine (140 mg, 0.5 mmol) was hydrogenated over Pd (5% on C, 50% wet, 40 mg) in ethanol (5 ml) for 16 hours. The catalyst was filtered off and the solvent removed under reduced pressure to afford the title compound as a brown oil. MS (m/z)=239 (M+H+); Calc'd for C13H22N2O2=238.33
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08557996B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-8137136def2144f8a731ddf5a9be39de |
| Source note | uspto-grants-2013_10 |