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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1042712Generated: November 1, 2026

N,N-Diethyl-2-(3-methoxy-4-nitrophenoxy)ethylamine → HCID 59428024, compound

https://huagongshe.com/reaction/1042712

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN,N-Diethyl-2-(3-methoxy-4-nitrophenoxy)ethylamineHCID 68463557—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 59428024HCID 59428024—

Reaction Steps

N,N-Diethyl-2-(3-methoxy-4-nitrophenoxy)ethylamine (140 mg, 0.5 mmol) was hydrogenated over Pd (5% on C, 50% wet, 40 mg) in ethanol (5 ml) for 16 hours. The catalyst was filtered off and the solvent removed under reduced pressure to afford the title compound as a brown oil. MS (m/z)=239 (M+H+); Calc'd for C13H22N2O2=238.33

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08557996B2
Source datasetuspto-grants-2013_10
ORD IDord-8137136def2144f8a731ddf5a9be39de
Source noteuspto-grants-2013_10