HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 68666651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 67145179 | HCID 67145179 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68666651 | HCID 68666651 | — |
Reaction Steps
N-Chloro-succinimide (160 mg) was added portionwise to a solution of EXAMPLE 265A (300 mg) in toluene (10 mL) and the mixture was stirred at room temperature for about two hours. The mixture was chromatographed on a silica gel column with 30% ethyl acetate in hexane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08557983B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-32ad3e2e231d4db8927eb9d14b6c43fe |
| Source note | uspto-grants-2013_10 |