huagongshe.com
HRID1043277

反应详情

EQUATION

反应方程式

HRID 1043277 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OB(c2ccc(N)cc2)OC1(C)C
HCID2734620

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

C12H18BNO2

结构：CC(C)(C)OC(=O)N1CC=C(OS(=O)(=O)C(F)(F)F)CC1
HCID10991161

tert-Butyl 4-[(trifluoromethanesulfonyl)oxy]-3,6-dihydropyridine-1(2H)-carboxylate

C11H16F3NO5S

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CC=C(c2ccc(N)cc2)CC1
HCID53415310

tert-Butyl 4-(4-aminophenyl)-3,6-dihydropyridine-1(2H)-carboxylate

C16H22N2O2

PROCEDURE

实验过程

The title compound was prepared by Suzuki coupling of 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenylamine with 4-trifluoromethanesulfonyloxy-3,6-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester (Synthesis, 993, (1991)) according to the procedure in Example 35, step (b). Mass spectrum (ESI, m/z): Calcd. for C16H22N2O2, 275.2 (M+H). found 275.1.