HCID 44125480, compound → HCID 19708208, compound

HRID 1043396Notes

Reaction equation

HRID 1043396 reaction equation
[CH:1]1([NH:7][C:8]2[C:13](CC(C)C)=[CH:12][C:11](CC(C)C)=[C:10]([NH:22][CH:23]3[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]3)[CH:9]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C1(NC2C(CC(C)C)=CC(C=C(C)C)=C(NC3CCCCC3)C=2)CCCCC1>>[CH:23]1([NH:22][C:10]2[CH:11]=[CH:12][CH:13]=[C:8]([NH:7][CH:1]3[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]3)[CH:9]=2)[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]1

Participants

3

Reactant 2

HCID 44125480HCID 44125480, compoundHCID 44125481HCID 44125481, compound

Product 1

HCID 19708208HCID 19708208, compound

Procedure

Recrystallization from ethyl acetate provided an off-white product, mp 92-94° C., containing 42% of N1,N3-dicyclohexyl-4,6-diisobutyl-1,3-benzenediamine, along with 35% N1,N3-dicyclohexyl-4-isobutenyl-6-isobutyl-1,3-benzenediamine, as determined by GC/MS.

Workup

  1. customRecrystallization from ethyl acetate
  2. customprovided an off-white product, mp 92-94° C.

Sources & evidence

ORD record
ord-b5136b0661d94d749a61755b8cbce4a1
Source dataset
uspto-grants-2013_10
Patent number
US08563489B2

Reaction notes

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