1,1-Bis(methylthio)-2-nitroethylene → N-((6-chloropyridin-3-yl)methyl)-N-ethyl-1-(methylthio)-2-nitroethenamine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	1,1-Bis(methylthio)-2-nitroethylene	HCID 83623	—
Edukt	N-((6-chloropyridin-3-yl)methyl)ethenamine	HCID 86658943	—
Lösungsmittel	Ethanol	HCID 702	—
Produkt	N-((6-chloropyridin-3-yl)methyl)-N-ethyl-1-(methylthio)-2-nitroethenamine	HCID 54422628	—

Reaktionsschritte

A mixture of N-((6-chloropyridin-3-yl)methyl)ethenamine and 1,1-dimethylthio-2-nitroethene is dissolved in ethanol and refluxed for 4-8 hours. After completion, the mixture is concentrated and purified by column chromatography to obtain N-((6-chloropyridin-3-yl)methyl)-N-ethyl-1-(methylthio)-2-nitroethenamine.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08563546B2
Quelldatensatz	uspto-grants-2013_10
ORD ID	ord-6bc09805537549f8830da3c2baad82a1
Quellennotiz	uspto-grants-2013_10