HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178513424, compound → HCID 58148007, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178513424 | HCID 178513424 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 58148007 | HCID 58148007 | 75.5% |
Reaction Steps
The solution of the product of example 21 (261 mg, 0.49 mmol) in toluene (5 ml) was heated at reflux for 2 h. After cooled to room temperature, the solids were collected by filtration, washed with diethyl ether and dried to give the titled product (190 mg, yield 75.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08563562B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-78bc28a13f394d488c07b41b97e71d2f |
| Source note | uspto-grants-2013_10 |