HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58126947, compound → 1202897-25-3
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58126947 | HCID 58126947 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 1202897-25-3 | HCID 66922414 | 135.6% |
Reaction Steps
A mixture of the product of example 29 (2.5 g, 10.53 mmol) with hydrochloride acid (6 mol/l, 30 ml) was refluxed for about 3 hours and then cooled to room temperature. The solids were collected by filtration, washed with EA and dried to give the titled product (1.7 g, 81%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08563562B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-95888caccafb478fa61702dcb867e71e |
| Source note | uspto-grants-2013_10 |