Methanol → HCID 58580204, compound

Participants

Reaction Steps

To a solution of 4-(hydroxymethyl)-1-(3-methoxy-4-((2-(trimethylsilyl)ethoxy)-methoxy)phenyl)pyridin-2(1H)-one Part E of Procedure 1 (900 mg, 2.38 mmol) in CH2Cl2 (10 mL) and MeOH (10 mL) was added 4M HCl/Dioxane (10.7 mL, 43 mmol). After stirring at RT for 1 h, concentration under vacuum provided the crude phenol as a white solid. LC-MS, [M+H]+=428.

Provenance & Evidence