HuagongsheHuagongshe Chemistry Print Report · For research reference only
Itaconic acid → HCID 86617348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Itaconic acid | HCID 811 | — |
| Reactant | Pentaerythritol | HCID 8285 | — |
| Reactant | Betulin | HCID 72326 | — |
| Reactant | L-Lactic Acid | HCID 107689 | — |
| Product | HCID 86617348 | HCID 86617348 | — |
Reaction Steps
Polymerisation was performed as in Example 3, but the amounts of ingredients were following: 85.2 g of L-lactic acid (78 mole-%), 25.9 g of itaconic acid (16.5 mole-%), 1.4 g of pentaerythritol (0.8 mole-%), 25 g of betulin (4.7 mole-%) and 0.0375 g of tin(II)octoate. Total polymerisation time was 20 hours. As product, was obtained hard brittle brownish yellow mass, which was end-functionalised according to the example 11 and finally crosslinked by radicals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08563664B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-b39e7badbc284a68b0b6902829ecabb0 |
| Source note | uspto-grants-2013_10 |