Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chlorobenzene | HCID 7964 | — |
| Reactant | 112110-17-5 | HCID 11182791 | — |
| Product | HCID 46899675 | HCID 46899675 | — |
Reaction Steps
106.8 g (0.65 mol) of 5-methyl-2,3-pyridine dicarboxylic acid anhydride were dissolved in 427 g chlorobenzene and heated up to 85° C. A solution of 0.64 g (0.004 mol) AlBN in 99.0 g (0.66 mol) SO2Cl2 was added during 45 min. The mixture was stirred for additional 90 min at 85° C. Chlorobenzene was partly distilled off and the solution was cooled to 10° C. via 10 h ramp. The precipitate was filtered off and washed with chlorobenzene/hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08563734B2 |
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| Source dataset | uspto-grants-2013_10 |
|---|
| ORD ID | ord-08789702294f4df69f98393bce106728 |
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| Source note | uspto-grants-2013_10 |
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