Thioguaiacol → HCID 10891209, compound

HRID 1045330Notes

Reaction equation

HRID 1045330 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[SH:9].[Cl:10][C:11]1[CH:18]=[C:17](F)[CH:16]=[CH:15][C:12]=1[CH:13]=[O:14]>>[Cl:10][C:11]1[CH:18]=[C:17]([S:9][C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[O:2][CH3:1])[CH:16]=[CH:15][C:12]=1[CH:13]=[O:14]

Participants

3

Reactant 2

HCID 23642ThioguaiacolHCID 1450242-Chloro-4-fluorobenzaldehyde

Product 1

HCID 10891209HCID 10891209, compound

Procedure

The target product (5.50 g) was obtained as a colorless oil by reacting 2-methoxybenzenethiol (2.80 g) and 2-chloro-4-fluorobenzaldehyde (3.17 g) based on the same experiment operations as in Reference Example 1 of WO 03029205 pamphlet.

Sources & evidence

ORD record
ord-dd166f2040394502836873202049c688
Source dataset
uspto-grants-2013_10
Patent number
US08569270B2

Reaction notes

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