HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3'-Methylcinnamanilide → 7-Methyl-2-quinolone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3'-Methylcinnamanilide | HCID 583018 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 7-Methyl-2-quinolone | HCID 77673 | 903,9% |
Reaktionsschritte
N-m-tolylcinnamamide (2 g, 0.834 mmol) and AlCl3 (1.12 g, 0.834 mmol) were heated for 1 h at 100° C. Water was added and the solid was filtered to provide 1.2 g of crude product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08569282B2 |
| Quelldatensatz | uspto-grants-2013_10 |
| ORD ID | ord-7f1b868a4e934450bb52fa07c8592317 |
| Quellennotiz | uspto-grants-2013_10 |