HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 67411117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Azide | HCID 33558 | — |
| Reactant | 3-Benzoyl-2-(2-bromo-2-methylpropanoylamino)-thiophene | HCID 67411846 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67411117 | HCID 67411117 | 65% |
Reaction Steps
3.4 g of the compound of Example 1 was boiled with sodium azide in ethanol under reflux. The crude azide was directly reduced with zinc and ammonium chloride in boiling ethanol to give 65% of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569288B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-e4f7f6edef2f428f818ba708b14fe810 |
| Source note | uspto-grants-2013_10 |