HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-chloro-3-isocyanato- → HCID 70496752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-chloro-3-isocyanato- | HCID 17968 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 70498061 | HCID 70498061 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 70496752 | HCID 70496752 | — |
Reaction Steps
57 (20 mg, 0.05 mmol), DIEA (304, 0.15 mmol), and 3-chlorophenyl isocyanate (9.4 mg, 0.06 mmol) were suspended in dioxane (2 mL), and stirred overnight at room temperature. The crude product was purified directly via HPLC. LC-MS (M+H=548, obsd.=548).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569295B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-366e46d251d34e068999ff16015e8cdc |
| Source note | uspto-grants-2013_10 |