Lithium Hydroxide → HCID 86685839, compound

Participants

Reaction Steps

The product from step A (41 mg, 0.116 mmol) in THF (2.0 ml) was treated with 1M aqueous LiOH (0.349 ml, 0.349 mmol) at rt. The mixture was stirred at rt for 12 h, poured into 2M aq NaHSO4 and extracted with MTBE. The combined organics were dried with anhydrous Na2SO4, filtered and concentrated to afford the title compound which was used without further purification. HPLC/MS: 339.1/340.9 (M+1); Rt=1.16 min (LC2).

Provenance & Evidence