HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-amino-4-fluoro-N-methoxybenzamide → HCID 58336569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-amino-4-fluoro-N-methoxybenzamide | HCID 64974609 | — |
| Reactant | N-(1,3-dimethylpyrazol-5-yl)-4-iodo-5-(trifluoromethyl)pyridin-2-amine | HCID 67075489 | — |
| Product | HCID 58336569 | HCID 58336569 | — |
Reaction Steps
This compound was prepared from N-(1,3-dimethylpyrazol-5-yl)-4-iodo-5-(trifluoromethyl)pyridin-2-amine and 2-amino-4-fluoro-N-methoxybenzamide. 81 mg, 48%; triturated in Et2O; NMR Spectrum: (DMSOd6) 2.08 (s, 3H), 3.55 (s, 3H), 3.70 (s, 3H), 6.04 (s, 1H), 6.74 (s, 1H), 6.97 (ddd, 1H), 7.43 (dd, 1H), 7.66 (dd, 1H), 8.28 (s, 1H), 9.07 (s, 1H), 10.04 (bs, 1H), 11.96 (bs, 1H); Mass spectrum: MH+ 439.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569298B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-a186298a208b4f2ba8b464ac625f960a |
| Source note | uspto-grants-2013_10 |