HRID1046042
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To 1000 ml of ethanol was added 120 g of Lamivudine oxalate (prepared by the method of the present invention). 60 ml of triethylamine was added at the temperature of 40˜45° C. for 0.5 hour, stirred at the same temperature for 4 hours, and centrifuged at room temperature. The product was dried under vacuum at the temperature of 40˜45° C. to obtain Lamivudine crystal.
WORKUP
后处理
- customprepared by the method of the present invention)
- customcentrifuged at room temperature
- customThe product was dried under vacuum at the temperature of 40˜45° C.