HRID1046042

反应详情

EQUATION

反应方程式

HRID 1046042 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To 1000 ml of ethanol was added 120 g of Lamivudine oxalate (prepared by the method of the present invention). 60 ml of triethylamine was added at the temperature of 40˜45° C. for 0.5 hour, stirred at the same temperature for 4 hours, and centrifuged at room temperature. The product was dried under vacuum at the temperature of 40˜45° C. to obtain Lamivudine crystal.

WORKUP

后处理

  1. customprepared by the method of the present invention)
  2. customcentrifuged at room temperature
  3. customThe product was dried under vacuum at the temperature of 40˜45° C.