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HRID1046095

反应详情

EQUATION

反应方程式

HRID 1046095 的结构方程式

REACTANTS

反应物

2
结构：C[C@@H](c1ccc(Br)cc1)N1CC[C@](CC(C)(C)O)(c2ccccc2)OC1=O
HCID44599033

未命名化合物

结构：CC1(C)OB(c2cccc(OC3CCCC3)n2)OC1(C)C
HCID45785773

2-(Cyclopentyloxy)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

C16H24BNO3

PRODUCTS

生成物

1
结构：C[C@@H](c1ccc(-c2cccc(OC3CCCC3)n2)cc1)N1CC[C@](CC(C)(C)O)(c2ccccc2)OC1=O
HCID58485373

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from (S)-3-((S)-1-(4-bromophenyl)ethyl)-6-(2-hydroxy-2-methylpropyl)-6-phenyl-1,3-oxazinan-2-one and 2-(cyclopentyloxy)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine following a procedure analogous to that described in Example 14. LC-MS Method 1 tR=2.23 min, m/z=515, 457; 1H NMR (CD3OD) 0.96 (s, 3H), 1.27 (s, 3H), 1.56 (d, 3H), 1.70 (2H), 1.85 (4H), 2.05 (2H), 2.17 (s, 2H), 2.24 (m, 1H), 2.46 (2H), 3.05 (m, 1H), 5.47 (m, 1H), 5.58 (q, 1H), 6.70 (d, 1H), 7.00 (d, 2H), 7.25-7.40 (6H), 7.70 (t, 1H), 7.77 (d, 2H).