HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1,3,5-trimethylpyrazole → HCID 46865841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1,3,5-trimethylpyrazole | HCID 519181 | — |
| Reactant | (S)-6-(2-hydroxy-2-methylpropyl)-6-phenyl-3-((S)-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethyl)-1,3-oxazinan-2-one | HCID 59532385 | — |
| Product | HCID 46865841 | HCID 46865841 | — |
Reaction Steps
The title compound was prepared from (S)-6-(2-hydroxy-2-methylpropyl)-6-phenyl-3-[(S)-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethyl]-1,3-oxazinan-2-one and 4-bromo-1,3,5-trimethyl-1H-pyrazole following a procedure analogous to that described in Example 171. Mass spectrum (ESI+): m/z=462 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569292B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-128bb67fb4ae43b8b5510486cadf5007 |
| Source note | uspto-grants-2013_10 |