2-Fluoro-4-iodopyridine → Pyridine, 4-iodo-2-(methylthio)-

HRID 1046244Notes

Reaction equation

HRID 1046244 reaction equation
F[C:2]1[CH:7]=[C:6]([I:8])[CH:5]=[CH:4][N:3]=1.BrC1C=[C:14]([S:16]C)C=CN=1>>[I:8][C:6]1[CH:5]=[CH:4][N:3]=[C:2]([S:16][CH3:14])[CH:7]=1

Participants

3

Reactant 2

HCID 70235702-Fluoro-4-iodopyridineHCID 234370172-Bromo-4-(methylthio)pyridine

Product 1

HCID 58485338Pyridine, 4-iodo-2-(methylthio)-

Procedure

The title compound was prepared from 2-fluoro-4-iodo-pyridine following a procedure analogous to that described for 2-bromo-4-methylsulfanyl-pyridine in Example 184. Mass spectrum (ESI+): m/z=252 [M+H]+.

Sources & evidence

ORD record
ord-bc8f9128d81146b1a281f2775747612e
Source dataset
uspto-grants-2013_10
Patent number
US08569292B2

Reaction notes

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