2-Bromo-6-(methylthio)pyridine → HCID 13275581, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([S:8][CH3:9])[N:3]=1.BrC1C=CC(S(C)=[O:18])=NC=1>>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([S:8]([CH3:9])=[O:18])[N:3]=1Participants
3
Procedure
The title compound was prepared from 2-bromo-6-methylsulfanyl-pyridine following a procedure analogous to that described for 5-bromo-2-methanesulfinyl-pyridine in Example 182. Mass spectrum (ESI+): m/z=220/222 (Br) [M+H]+.
Sources & evidence
- ORD record
- ord-eef52a12d82548ef8ab5e1d9334d2d5c
- Source dataset
- uspto-grants-2013_10
- Patent number
- US08569292B2
Reaction notes
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