HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanate → HCID 59259078, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanate | HCID 517096 | — |
| Reactant | Water ethylacetate | HCID 22728543 | — |
| Reactant | HCID 59259032 | HCID 59259032 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59259078 | HCID 59259078 | — |
Reaction Steps
A solution of 338 mg (0.72 mmol) of the product prepared in step C in 6 ml AcOH is treated with 70 mg (1.1 mmol) sodium cyanate. The mixture is stirred for 1.5 h at rt. A yellow product results after work-up with ethyl acetate/water, which is purified by chromatography (CH2Cl2/MeOH) to afford a yellow foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569317B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-c0944e24750c4e37bc4ce97799321b03 |
| Source note | uspto-grants-2013_10 |