Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Ethyl 4-bromobenzimidate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Benzonitrile, 4-bromo- | HCID 12162 | — |
| 생성물 | Ethyl 4-bromobenzimidate hydrochloride | HCID 19017302 | 99% |
반응 단계
A solution of 4-bromobenzonitrile (17.65 g, 97 mmol) in ethanol (500 mL) was acidified with hydrogen chloride gas at 0° C. for fifteen minutes. The solution was allowed to stir for 16 h. The solution was condensed under reduced pressure to afford the title compound (25.35 g, 99%). MS (ESI) m/z 228.1 [M]+, 230.4 [M+2]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08569494B2 |
| 출처 데이터셋 | uspto-grants-2013_10 |
| ORD ID | ord-3b21494f3b9542b29a5535197a7bf9e5 |
| 출처 메모 | uspto-grants-2013_10 |