Morpholine → HCID 53994124, compound

HRID 1047351Notes

Reaction equation

HRID 1047351 reaction equation
C1([N:7]2[CH2:12][CH2:11][O:10][CH2:9][CH2:8]2)CCCCC=1.[CH3:13][C:14]1([CH3:21])[CH2:19][CH2:18][C:17](=O)[CH2:16][CH2:15]1.N1CCOCC1>C1CCCCC1>[CH3:13][C:14]1([CH3:21])[CH2:19][CH2:18][C:17]([N:7]2[CH2:12][CH2:11][O:10][CH2:9][CH2:8]2)=[CH:16][CH2:15]1

Participants

5

Reactant 3

HCID 8083MorpholineHCID 69589Morpholine, 4-(1-cyclohexen-1-yl)-HCID 138166Cyclohexanone, 4,4-dimethyl-

Product 1

HCID 53994124HCID 53994124, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

Compound III″ (brown liquid) is obtained quantitatively according to Example 1, from 4,4-dimethylcyclohexanone (350.03 g, 2.76 mol), morpholine (327.01 g, 3.75 mol) and cyclohexane (330 mL).

Sources & evidence

ORD record
ord-32431e47f0d34865bd507e2279424f86
Source dataset
uspto-grants-2013_10
Patent number
US08569518B2

Reaction notes

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