HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → Diisobutyl aluminium azide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Diisobutyl aluminium chloride | HCID 16686353 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Diisobutyl aluminium azide | HCID 86610998 | — |
Reaction Steps
1.235 g of granular sodium azide (19 mmol) are added to a cold solution of diisobutyl aluminium chloride (19 mmol, 1.8M in toluene) diluted in 5 ml of toluene and the mixture is stirred at room temperature over the night to give diisobutyl aluminium azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569528B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-64e4130e48684bdfb9deb439bc89815c |
| Source note | uspto-grants-2013_10 |