HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphosgene → HCID 89875585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | 3-Ethoxy-2-methylaniline | HCID 13737011 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 89875585 | HCID 89875585 | 249.2% |
Reaction Steps
At room temperature, to a mixture of 3-ethoxy-2-methylaniline 33.0 g and toluene 400 mL was added triphosgene 25 g, and the resulting mixtures were stirred with heating reflux for four hours. The mixtures were concentrated under reduced pressure to give 1-ethoxy-3-isocyanato-2-methylbenzene 37.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09380782B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-e076b4e41619415e804851e0821c341d |
| Source note | uspto-grants-2016_07 |