Water → HCID 68176657, compound

Participants

Reaction Conditions

Reaction Steps

5,7-Dihydroxymethylchromone (15 g, 78 mmol) is dissolved in N,N-dimethylformamide (360 ml), and potassium tert-butoxide (9 g, 80 mmol) is added to the brown solution under a stream of nitrogen. The mixture is subsequently heated at 30° C. for 2.5 h. Palmitoyl chloride (24 ml, 79.5 mmol) in N,N-dimethylformamide (80 ml) is then slowly added dropwise to the solution at 30° C. The resultant suspension is stirred at 30° C. for a further 2 hours, and 400 ml of DI water are then added dropwise. After 1 hour, the solid is filtered off with suction via a suction filter, dried well by suction and dried at 40° C. in a vacuum drying cabinet.

Provenance & Evidence