2-Fluoro-5-(methylamino)-4-nitrobenzonitrile → HCID 66684554, compound

Participants

Reaction Steps

A stirred solution of 2-Fluoro-5-methylamino-4-nitro-benzonitrile (1.0 g, 0.0051 mol) in EtOH (20 mL) was hydrogenated using Pd/C for 3 h at room temperature. The reaction was filtered through CELITE® and the filter bed was thoroughly washed with EtOH. The resulting solution was concentrated to afford the crude 4-amino-2-fluoro-5-methylamino-benzonitrile as a brownish black solid. C8H8FN3; Crude LCMS (M+1): 166.2; LCMS Purity: 85.05%.

Provenance & Evidence