HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → (3,3-Dimethylbutyl)(triphenyl)phosphonium methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 3,3-Dimethylbutyl methanesulfonate | HCID 19039459 | — |
| Product | (3,3-Dimethylbutyl)(triphenyl)phosphonium methanesulfonate | HCID 85243721 | 98.2% |
Reaction Steps
3,3-Dimethylbutyl methanesulfonate (36.5 g) and triphenylphosphine (53.1 g) were stirred at 120° C. for 15 hr to give the title compound (88.0 g) as a white gummy substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382188B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-b89aa59b3b0e4ed5a4d28a1455d38872 |
| Source note | uspto-grants-2016_07 |