HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorophenyl isocyanate → HCID 117699222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorophenyl isocyanate | HCID 76833 | — |
| Reactant | 5-(4-Aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione | HCID 117699167 | — |
| Product | HCID 117699222 | HCID 117699222 | 40.3% |
Reaction Steps
By using 5-(4-aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione (32 mg, 0.10 mmol) obtained in Example 1, (3), and 2-chlorophenyl isocyanate (30 μL, 0.25 mmol), the title compound (19 mg, yield 40%) was obtained in the same manner as that of Example 20.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-6d2a4d4932a74a7f85d091337d85752a |
| Source note | uspto-grants-2016_07 |