HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,4-Dichlorophenoxy)Acetic Acid → HCID 117699254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,4-Dichlorophenoxy)Acetic Acid | HCID 1486 | — |
| Reactant | (2,4-Dichlorophenoxy)acetyl chloride | HCID 69887 | — |
| Reactant | 5-(4-Aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione | HCID 117699167 | — |
| Product | HCID 117699254 | HCID 117699254 | 22.3% |
Reaction Steps
2,4-Dichlorophenoxyacetic acid (42 mg, 0.190 mmol) was made into acid chloride in a conventional manner. By using 5-(4-aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione (30 mg, 0.095 mmol) obtained in Example 1, (3), and 2,4-dichlorophenoxyacetic acid chloride mentioned above, the title compound (11 mg, yield 22%) was obtained in the same manner as that of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-fb56535e76b14badbcd7a699065a847c |
| Source note | uspto-grants-2016_07 |