HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzofuran-2-carboxylic acid → HCID 117699210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzofuran-2-carboxylic acid | HCID 10331 | — |
| Reactant | 2-Benzofurancarbonyl chloride | HCID 38949 | — |
| Reactant | 5-(4-Aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione | HCID 117699167 | — |
| Product | HCID 117699210 | HCID 117699210 | 101.5% |
Reaction Steps
Benzofuran-2-carboxylic acid (31 mg, 0.189 mmol) was made into acid chloride in a conventional manner. By using 5-(4-aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione (40 mg, 0.126 mmol) obtained in Example 1, and benzofuran-2-carboxylic acid chloride mentioned above, the title compound (59 mg, yield 100%) was obtained in the same manner as that of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-2a49f44a62df41138b68b97f091ee5fd |
| Source note | uspto-grants-2016_07 |