HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanedioyl dichloride → HCID 117699333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanedioyl dichloride | HCID 74269 | — |
| Reactant | 4-Bromo-3-methyl-2-nitrophenol | HCID 13088179 | — |
| Reactant | HCID 117699223 | HCID 117699223 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 117699333 | HCID 117699333 | 10.6% |
Reaction Steps
N-[4-(2-Amino-4-bromo-3-methylphenylamino)phenyl]benzenesulfonamide (100 mg, 0.231 mmol) synthesized by using 4-bromo-3-methyl-2-nitrophenol was treated with malonyl chloride (22 μL, 0.226 mmol) in THF to give the title compound (12 mg, yield 10%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-4e4ece57979d46d9b8733905773bc406 |
| Source note | uspto-grants-2016_07 |