HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium p-toluenesulfinate → HCID 73442307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium p-toluenesulfinate | HCID 2723791 | — |
| Reactant | HCID 73442187 | HCID 73442187 | — |
| Product | HCID 73442307 | HCID 73442307 | — |
Reaction Steps
50 mg (138 μmol) 6-[(6-bromo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)amino]-1,3-benzothiazol-2(3H)-one (prepared according to example 8) were transformed in analogy to intermediate example 23 using sodium 4-methylbenzenesulfinate to give after working up and purification 6.7 mg (11%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382255B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-1b9f8c03fa68436ebd0ff67312f63fb9 |
| Source note | uspto-grants-2016_07 |