HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 89429115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 4-Acetylpyridine | HCID 14282 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 89429115 | HCID 89429115 | — |
Reaction Steps
2.0 g 4-Acetylpyridine were dissolved in 10 ml acetonitrile and 2.0 g dimethyl sulfate were added. After refluxing for 5 h, the solution was added dropwise to 40 ml ethyl acetate and the precipitate was filtered, washed with ethyl acetate and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382278B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-c860a426915c42c68774466b3b3139a5 |
| Source note | uspto-grants-2016_07 |