Ammonium dithiocarbamate → HCID 178480225, compound

HRID 1049976Notes

Reaction equation

HRID 1049976 reaction equation
[C:1](=[S:4])([S-:3])[NH2:2].[NH4+].[Br-].[Br:7][CH2:8][C:9]([C:11]1[CH:16]=[CH:15][N+:14]([CH3:17])=[CH:13][CH:12]=1)=O>CO>[Br-:7].[CH3:17][N+:14]1[CH:15]=[CH:16][C:11]([C:9]2[N:2]=[C:1]([SH:3])[S:4][CH:8]=2)=[CH:12][CH:13]=1

Participants

4

Reactant 2

HCID 11083854Ammonium dithiocarbamateHCID 89428956HCID 89428956, compound

Product 1

HCID 178480225HCID 178480225, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

0.69 g Ammonium dithiocarbamate were dissolved in 10 ml MeOH and 1.47 g 4-(2-bromoacetyl)-1-methylpyridinium bromide were added. After 2 h at ambient temperature the mixture was refluxed. After cooling the precipitate was filtered, washed with MeOH and dried.

Workup

  1. temperatureAfter cooling the precipitate
  2. filtrationwas filtered
  3. washwashed with MeOH
  4. customdried

Sources & evidence

ORD record
ord-ffce9b7afdfc4893a049d39cae922535
Source dataset
uspto-grants-2016_07
Patent number
US09382278B2

Reaction notes

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