HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 90295829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 90295823 | HCID 90295823 | — |
| Product | HCID 90295829 | HCID 90295829 | 85.8% |
Reaction Steps
Using compound (3R,3aS)-3-(((t-butyldimethylsilyl)oxy)methyl)-7-(2-oxopiperidin-1-yl)-3a,4-dihydrobenzo[b]oxazolo[3,4-d][1,4]oxazin-1(3H)-one (1.016 g, 2.352 mmol), and tetra-n-butylammonium fluoride (1M, 4.7 ml) as starting materials, preparation following the method as described in Example 1(b) afforded 0.642 g white solid, yield 85.8%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382265B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-d63b811209bb4700a1db8b123a411cc4 |
| Source note | uspto-grants-2016_07 |