HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 90295548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 90295754 | HCID 90295754 | — |
| Product | HCID 90295548 | HCID 90295548 | 86.53% |
Reaction Steps
Using N-((3R,3aS)-3-(((t-butyldimethylsilyl)oxy)methyl)-1-oxo-1,3,3a,4-tetrahydrobenzo[b]oxazolo[3,4-d][1,4]oxazin-7-yl)-N-methylacetamide (0.617 g, 1.52 mmol), and TBAF (1M, 2 ml) as starting materials, preparation following the method as described in Example 1 (b) afforded white solid 0.384 g, yield: 86.53%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382265B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-15745ce627524881a59f3c377ca2c6d8 |
| Source note | uspto-grants-2016_07 |