Tetraethyltin → HCID 136344068, compound

HRID 1050816Notes

Reaction equation

[CH2:1]([O:5][C:6]([C:8]1[C:9]([OH:19])=[C:10]2[C:17]([CH3:18])=[N:16][S:15][C:11]2=[C:12](Br)[N:13]=1)=[O:7])[CH2:2][CH2:3][CH3:4].[CH2:20]([Sn](CC)(CC)CC)[CH3:21]>>[CH2:1]([O:5][C:6]([C:8]1[C:9]([OH:19])=[C:10]2[C:17]([CH3:18])=[N:16][S:15][C:11]2=[C:12]([CH2:20][CH3:21])[N:13]=1)=[O:7])[CH2:2][CH2:3][CH3:4]

Participants

Reactant 2

HCID 11704Tetraethyltin

HCID 136343979HCID 136343979, compound

Product 1

HCID 136344068HCID 136344068, compound

Procedure

The title compound was synthesized in analogy to Example 28 from 7-bromo-4-hydroxy-3-methyl-isothiazolo[5,4-c]pyridine-5-carboxylic acid butyl ester and tetraethyltin: MS (m/z) 295.2 (M+1).

Sources & evidence

ORD record: ord-a60268ceb0fc4f9e9b6cf2ead09f1038
Source dataset: uspto-grants-2016_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09387200B2

Reaction notes

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