HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → (E)-Parinaric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl | HCID 11269872 | — |
| Product | (E)-Parinaric acid | HCID 5282838 | — |
Reaction Steps
The machine was equipped with a deprotection tube (empty, but used for sparging the MIDA boronate solution) and a reaction tube charged with the Pd-mixture (60 mg), the SPhos-mixture (60 mg), KOH (75 mg, 1.7 mmol) and halide 3 (11 mg, 0.037 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388131B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-5f6615cba0844fea9229613c7cd3b157 |
| Source note | uspto-grants-2016_07 |