HRID1051055

反应详情

EQUATION

反应方程式

HRID 1051055 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a stirred solution of (R)- or (S)-indane amine (1 eq) in DCM (0.05M) was added TEA (2 eq) and the appropriate sulfonyl chloride (2 eq.) at room temperature. The reaction mixture was stirred at room temperature for 18 h. The solvent was evaporated and the pure product isolated after preparative HPLC purification.

WORKUP

后处理

  1. customat room temperature
  2. customThe solvent was evaporated
  3. customthe pure product isolated
  4. customafter preparative HPLC purification