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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1051171Generated: November 3, 2026

HCID 88963060, compound → HCID 68386890, compound

https://huagongshe.com/reaction/1051171

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 88963060HCID 88963060—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
SolventTetrahydrofuranHCID 8028—
ProductHCID 68386890HCID 6838689081.2%

Reaction Conditions

Temperature23 °C

Reaction Steps

To a solution of 80 mg (309 μmol) 3,5-dinitrobiphenyl-4-amine in a mixture of 34 mL ethanol and 10 mL THF were added 6.6 mg palladium on charcoal (10%) and the mixture was stirred under an atmosphere of hydrogen for 26 hours at 23° C. After filtration and removal of the solvent the residue was purified by chromatography to yield 50 mg (81%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09388140B2
Source datasetuspto-grants-2016_07
ORD IDord-adf01b455d9442928b0661d0a5064a91
Source noteuspto-grants-2016_07