HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1051171Generated: November 3, 2026
HCID 88963060, compound → HCID 68386890, compound
https://huagongshe.com/reaction/1051171
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 88963060 | HCID 88963060 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68386890 | HCID 68386890 | 81.2% |
Reaction Steps
To a solution of 80 mg (309 μmol) 3,5-dinitrobiphenyl-4-amine in a mixture of 34 mL ethanol and 10 mL THF were added 6.6 mg palladium on charcoal (10%) and the mixture was stirred under an atmosphere of hydrogen for 26 hours at 23° C. After filtration and removal of the solvent the residue was purified by chromatography to yield 50 mg (81%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09388140B2 |
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| Source dataset | uspto-grants-2016_07 |
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| ORD ID | ord-adf01b455d9442928b0661d0a5064a91 |
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| Source note | uspto-grants-2016_07 |
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